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  • ASTM
    E396-12e1 Standard Test Methods for Chemical Analysis of Cadmium
    Edition: 2012
    $113.57
    Unlimited Users per year

Description of ASTM-E396 2012

ASTM E396 - 12e1

Standard Test Methods for Chemical Analysis of Cadmium

Active Standard ASTM E396 | Developed by Subcommittee: E01.05

Book of Standards Volume: 03.05




ASTM E396

Significance and Use

These test methods for the chemical analysis of cadmium are primarily intended to test such material for compliance with compositional specifications in Specification B440 . It is assumed that all who use these test methods will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory.

1. Scope

1.1 These test methods cover the chemical analysis of cadmium having chemical compositions with the following limits:

Element Composition, max, %
Antimony 0.001
Arsenic 0.003
Copper 0.015
Lead 0.025
Silver 0.010
Thallium 0.003
Tin 0.010
Zinc 0.035

1.2 The test methods appear in the following order:

Sections
Antimony by the Rhodamine B Spectrophotometric Method
[0.0002 % to 0.0010 %] 		62-72
Arsenic by the Molybdenum Blue Spectrophotometric Method
[0.001 % to 0.005 %] 		40-50
Copper by the Neocuproine Spectrophotometric Method [0.002 % to 0.030 %] 10-19
Copper, Lead, Silver, and Zinc by the Atomic Absorption Method [0.004 % to 0.02 % Cu, 0.01 % to 0.05 % Pb, 0.004 % to 0.02 % Ag
and 0.01 % to 0.05 % Zn] 		51-61
Lead by the Dithizone Spectrophotometric Method [0.001 % to 0.05 %] 20-29
Thallium by the Rhodamine B Spectrophotometric Method
[0.0003 % to 0.005%] 		30-39
Tin by the 8-Quinolinol Spectrophotometric Method [0.0025 % to 0.0150 %] 73-82

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary information is given in Section 6, 25.8, 35.2, and 35.3.


2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

ASTM Standards

B440 Specification for Cadmium

D1193 Specification for Reagent Water

E29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications

E50 Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials

E55 Practice for Sampling Wrought Nonferrous Metals and Alloys for Determination of Chemical Composition

E60 Practice for Analysis of Metals, Ores, and Related Materials by Spectrophotometry

E88 Practice for Sampling Nonferrous Metals and Alloys in Cast Form for Determination of Chemical Composition

E135 Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials

E173 Practice for Conducting Interlaboratory Studies of Methods for Chemical Analysis of Metals

E1601 Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method


Keywords

antimony; arsenic; atomic absorption; cadmium; copper; lead; silver; spectrophotometry; thallium; tin; zinc ;


ICS Code

ICS Number Code 71.040.40 (Chemical analysis); 77.040.30 (Chemical analysis of metals)


DOI: 10.1520/E0396-12E01

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ASTM E396

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ASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide.
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