ASTM E354-93(2000)e1
Historical Standard: ASTM E354-93(2000)e1 Standard Test Methods for Chemical Analysis of High-Temperature, Electrical, Magnetic, and Other Similar Iron, Nickel, and Cobalt Alloys
SUPERSEDED (see Active link, below)
ASTM E354
1. Scope
1.1 These test methods cover the chemical analysis of high-temperature, electrical, magnetic, and other similar iron, nickel, and cobalt alloys having chemical compositions within the following limits:
| Element | Concentration Range, % | ||
| Aluminum | 0.005 | to | 18.00 |
| Beryllium | 0.001 | to | 0.05 |
| Boron | 0.001 | to | 1.00 |
| Calcium | 0.002 | to | 0.05 |
| Carbon | 0.001 | to | 1.10 |
| Chromium | 0.10 | to | 33.00 |
| Cobalt | 0.10 | to | 75.00 |
| Columbium (Niobium) | 0.01 | to | 6.0 |
| Copper | 0.01 | to | 10.00 |
| Iron | 0.01 | to | 85.00 |
| Magnesium | 0.001 | to | 0.05 |
| Manganese | 0.01 | to | 3.0 |
| Molybdenum | 0.01 | to | 30.0 |
| Nickel | 0.10 | to | 84.0 |
| Nitrogen | 0.001 | to | 0.20 |
| Phosphorus | 0.002 | to | 0.08 |
| Silicon | 0.01 | to | 5.00 |
| Sulfur | 0.002 | to | 0.10 |
| Tantalum | 0.005 | to | 10.0 |
| Titanium | 0.01 | to | 5.00 |
| Tungsten | 0.01 | to | 18.00 |
| Vanadium | 0.01 | to | 3.25 |
| Zirconium | 0.01 | to | 2.50 |
1.2 The test methods in this standard are contained in the sections indicated below:
| Sections | |
| Aluminum, Total, by the 8-Quinolinol Gravimetric Method (0.20 to7.00 %) | 100 |
| Carbon,Total, by the Combustion-Thermal Conductivity Method | 1 a |
| Carbon, Total, by the Combustion Gravimetric Method (0.05 to1.10 %) | 79 |
| Chromium by the Atomic Absorption Method (0.006 to 1.00 %) | 165 |
| Chromium by the Peroxydisulfate Oxidation-Titration Method(0.10 to 33.00 %) | 175 |
| Chromium by the Peroxydisulfate-Oxidation Titrimetric Method | 1 b |
| Cobalt by the Ion-Exchange-Potentiometric Titration Method (2 to75 %) | 53 |
| Cobalt by the Nitroso-R-Salt Photometric Method (0.10 to 5.0 %) | 61 |
| Copper by Neocuproine Photometric Method (0.01 to 10.00 %) | 90 |
| Copper by the Sulfide Precipitation-Electrodeposition GravimetricMethod (0.01 to 10.00 %) | 71 |
| Iron by the Silver ReductionTitrimetric Method (1.0 to 50.0 %) | 192 |
| Manganese by the Periodate Photometric Method (0.05 to 2.00 %) | |
| Molybdenum by the Ion Exchange-8-Hydroxyquinoline Gravi-metric Method (1.5 to 30 %) | 184 |
| Molybdenum by the Photometric Method (0.01 to 1.50 %) | 153 |
| Nickel by the Dimethylglyoxime Gravimetric Method (0.1 to84.0 %) | 135 |
| Phosphorus by the Molybdenum Blue Photometric Method (0.002to 0.08 %) | 18 |
| Silicon by the Gravimetric Method (0.05 to 5.00 %) | 46 |
| Sulfur by the Gravimetric Method | 1 c |
| Sulfur by the Combustion-Iodate Titration Method (0.005 to0.1 %) | 37 |
| Sulfur by the Chromatographic Gravimetric Method | 1b |
| Tin by the Solvent Extraction-Atomic Absorption Method (0.002to 0.10 %) | 143 |
1.3 Methods for the determination of several elements not included in this standard can be found in Test Methods E30 and Test Methods E1019.
1.4 Some of the concentration ranges given in 1.1 are too broad to be covered by a single method and therefore this standard contains multiple methods for some elements. The user must select the proper method by matching the information given in the Scope and Interference sections of each method with the composition of the alloy to be analyzed.
1.5 The values stated in SI units are to be regarded as standard. In some cases, exceptions allowed in Practice E380 are also used.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 5 and in special 'Warning' paragraphs throughout these test methods.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
ASTM Standards
D1193 Specification for Reagent Water
E29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
E30 Test Methods for Chemical Analysis of Steel, Cast Iron, Open-Hearth Iron, and Wrought Iron
E50 Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials
E60 Practice for Analysis of Metals, Ores, and Related Materials by Spectrophotometry
E173 Practice for Conducting Interlaboratory Studies of Methods for Chemical Analysis of Metals
E350 Test Methods for Chemical Analysis of Carbon Steel, Low-Alloy Steel, Silicon Electrical Steel, Ingot Iron, and Wrought Iron
E351 Test Methods for Chemical Analysis of Cast Iron--All Types
E352 Test Methods for Chemical Analysis of Tool Steels and Other Similar Medium- and High-Alloy Steels
E353 Test Methods for Chemical Analysis of Stainless, Heat-Resisting, Maraging, and Other Similar Chromium-Nickel-Iron Alloys
E882 Guide for Accountability and Quality Control in the Chemical Analysis Laboratory
E1019 Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel, Iron, Nickel, and Cobalt Alloys by Various Combustion and Fusion Techniques
E1806 Practice for Sampling Steel and Iron for Determination of Chemical Composition
Other Document
ISO 5725 Precision of Test Methods--Determination of Repeatability and Reproducibility for Inter-Laboratory Tests Available from American National Standards Institute (ANSI), 25 W. 43rd St., 4th Floor, New York, NY 10036, http://www.ansi.org.Keywords
aluminum; chromium; cobalt; cobalt alloys; combustion analysis; copper; high temperature alloys; induction furnace; infrared absorption; iron; manganese; magnetic alloys; molybdenum; nickel; nickel alloys; phosphorus; silicon; sulfur; tin; total carbon;
ICS Code
ICS Number Code 77.140.40 (Steels with special magnetic properties)
DOI: 10.1520/E0354-93R00E01
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