ASTM D7111-05
Historical Standard: ASTM D7111-05 Standard Test Method for Determination of Trace Elements in Middle Distillate Fuels by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
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Translated Standard: Russian
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ASTM D7111
1. Scope
1.1 This test method covers the determination of selected elements in middle distillate fuels by inductively coupled plasma atomic emission spectrometry (ICP-AES). The specific elements are listed in . The concentration range of this test method is approximately 0.1 to 2.0 mg/kg. The test method may be used for concentrations outside of this range; however, the precision statements may not be applicable. Middle distillate fuels covered in this test method have all distillation fractions contained within the boiling range of 150 to 390C. This includes, but is not limited to, diesel fuels and aviation turbine fuels.
1.2 This test method is not intended to analyze insoluble particulates. However, very small particulate matter (smaller than a micrometre) will be carried into the plasma and be included in the quantitative analysis.
1.3 This test method may give a result that is higher than the true value if an analyte is present in the sample in a form which is sufficiently volatile. For example, hexamethyldisiloxane will generate a biased high result for silicon.
1.4 The values stated in SI units are to be regarded as standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
ASTM Standards
D2880 Specification for Gas Turbine Fuel Oils
D3605 Test Method for Trace Metals in Gas Turbine Fuels by Atomic Absorption and Flame Emission Spectroscopy
D4057 Practice for Manual Sampling of Petroleum and Petroleum Products
D4306 Practice for Aviation Fuel Sample Containers for Tests Affected by Trace Contamination
D5185 Test Method for Determination of Additive Elements, Wear Metals, and Contaminants in Used Lubricating Oils and Determination of Selected Elements in Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
D6299 Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
D6792 Practice for Quality System in Petroleum Products and Lubricants Testing Laboratories
D7260 Practice for Optimization, Calibration, and Validation of Inductively Coupled Plasma-Atomic Emission Spectrometry (ICP-AES) for Elemental Analysis of Petroleum Products and Lubricants
Military Standard
MIL-F-16884J Military Specification, Fuel, Naval Distillate Naval Sea Systems Command (NAVSEA), SEA03R42, 1333 Isaac Hull Ave., SE, Washington, DC 20376.Keywords
aviation turbine fuel; diesel fuel; elemental analysis; fuel; ICP; inductively coupled plasma atomic emission spectrometry; internal standard; middle distillate fuels; trace elements: Borderline pumping temperature (BPT); Critical pumpability viscosity; Engine (lubricating) oils; Gelation; ICP-AES (inductively-coupled plasma atomic emission spectrometry); Middle distillate fuels; Scanning Brookfield technique; Viscosity;
ICS Code
ICS Number Code 75.160.20 (Liquid fuels)
DOI: 10.1520/D7111-05
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