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  • ASTM
    D4747-02(2014) Standard Test Method for Determining Unreacted Monomer Content of Latexes Using Gas-Liquid Chromatography
    Edition: 2014
    $82.37
    Unlimited Users per year

Description of ASTM-D4747 2014

ASTM D4747-02-Reapproved2014

Withdrawn Standard: Standard Test Method for Determining Unreacted Monomer Content of Latexes Using Gas-Liquid Chromatography (Withdrawn 2019)




ASTM D4747

Scope

1.1 This test method covers the determination of free monomer content of acrylic latexes. Monomers that have been successfully determined by this procedure include n-butyl methacrylate, n-butyl acrylate, styrene, and methyl methacrylate. The determination of other monomers has not been evaluated, but this test method is believed to be applicable. The established working range of this test method is from 100 to 1000 μg/g, but there is no reason to believe it will not work outside of this range, provided that appropriate dilutions and adjustments in specimen size are made.

1.2 The volatile composition of acrylic latexes is expected to change with time and environmental factors. This time dependence of the determination may be seen as an artificially large deviation of results, making the method mostly applicable for in-house quality control, where sampling and analysis conditions can be better controlled.

1.3 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See Section 7 for specific hazard statements.


Keywords

analysis of monomers; acrylic latexes chromatography (subheading gas chromatography); gas chromatography; latex paints; latex vehicles; styrene; trace monomers; unreacted monomers in latexes


ICS Code

ICS Number Code 83.040.10 (Latex and raw rubber)


DOI: 10.1520/D4747-02R14

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About ASTM

ASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide.
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