ASTM D4289-97
Historical Standard: ASTM D4289-97 Standard Test Method for Elastomer Compatibility of Lubricating Greases and Fluids
SUPERSEDED (see Active link, below)
ASTM D4289
1. Scope
1.1 This test method evaluates the compatibility of lubricating greases and fluids with coupons cut from standard elastomer sheets (Practice D3182) or, optionally, from SAE Specification AMS 3217/2A (NBR-L) and AMS 3217/3A (CR) sheets. Compatibility is evaluated by determining the changes in volume and Durometer A hardness that occur when elastomer coupons are totally immersed in a lubricant sample for 70 h at either 100 or 150 o C or as required by the lubricant specification.
1.1.1 Some lubricant specifications may require different test conditions, such as longer durations or lower or higher temperatures. In such instances, the repeatability and reproducibility values stated in Section 12 do not apply, and the user and supplier should agree on acceptable limits of precision.
Note 1--The scope of this test method now includes the evaluation of the elastomer compatibility of both lubricating fluids and greases. Testing of fluids was not included in Test Method D4289 - 95 and earlier versions.1.2 This test method can also be used as a guide to evaluate the compatibility of greases with rubber products not in standard sheet form (Practice D3183).
1.3 The values stated in SI and Durometer A units shall be regarded as the standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Note 6, Note 7, and Note 8.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
ASTM Standards
D217 Test Methods for Cone Penetration of Lubricating Grease
D297 Test Methods for Rubber Products--Chemical Analysis
D412 Test Methods for Vulcanized Rubber and Thermoplastic Elastomers--Tension
D471 Test Method for Rubber Property--Effect of Liquids
D1193 Specification for Reagent Water
D2240 Test Method for Rubber Property--Durometer Hardness
D3182 Practice for Rubber--Materials, Equipment, and Procedures for Mixing Standard Compounds and Preparing Standard Vulcanized Sheets
D3183 Practice for Rubber--Preparation of Pieces for Test Purposes from Products
D4175 Terminology Relating to Petroleum, Petroleum Products, and Lubricants
D4950 Classification and Specification for Automotive Service Greases
Federal Standards
Federal Test Method Method 3603.5, Swelling of Synthetic RubbersU.S. Air Force Specifications
USAF-539 Specification Bulletin for Standard Elastomer StocksSAE Standards
AMS 3217/3A Test Slabs, Chloroprene (CR)--65-75Keywords
compatibility; density; elastomer; fluid; grease; immersion; lubricant; lubricating grease; relative; rubber; seal(s); Compatibility--petroleum products; Elastomeric materials/applications; Hardness tests; Lubricating grease; Specific gravity--petroleum products; Volumetric measurement--petroleum products;
ICS Code
ICS Number Code 75.100 (Lubricants, industrial oils and related products)
DOI: 10.1520/D4289-97
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