ASTM D129-00(2005)
Historical Standard: ASTM D129-00(2005) Standard Test Method for Sulfur in Petroleum Products (General Bomb Method)
SUPERSEDED (see Active link, below)
ASTM D129
1. Scope
1.1 This test method covers the determination of sulfur in petroleum products, including lubricating oils containing additives, additive concentrates, and lubricating greases that cannot be burned completely in a wick lamp. The test method is applicable to any petroleum product sufficiently low in volatility that it can be weighed accurately in an open sample boat and containing at least 0.1 % sulfur.
Note 1This test method is not applicable to samples containing elements that give residues, other than barium sulfate, which are insoluble in dilute hydrochloric acid and would interfere in the precipitation step. These interfering elements include iron, aluminum, calcium, silicon, and lead which are sometimes present in greases, lube oil additives, or additive oils. Other acid insoluble materials that interfere are silica, molybdenum disulfide, asbestos, mica, and so forth. The test method is not applicable to used oils containing wear metals, and lead or silicates from contamination. Samples that are excluded can be analyzed by Test Method D 1552.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See 3.2 for specific precautionary directions incorporated in the test method.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
ASTM Standards
D1193 Specification for Reagent Water
D1552 Test Method for Sulfur in Petroleum Products (High-Temperature Method)
D6299 Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
E144 Practice for Safe Use of Oxygen Combustion Bombs
Keywords
high pressure decomposition device; sulfur;
ICS Code
ICS Number Code 75.080 (Petroleum products in general)
DOI: 10.1520/D0129-00R05
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