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eLibrary > BS ISO 4626:2023 Volatile organic liquids. Determination of boiling range of organic solvents used as raw materials >

BS ISO 4626:2023 Volatile organic liquids. Determination of boiling range of organic solvents used as raw materials, 2023

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Foreword
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Apparatus
6 Sampling
7 Assembly and preparation of apparatus [Go to Page]
7.1 Assembly [Go to Page]
7.1.1 General
7.1.2 Position and choice of thermometer
7.1.3 Support for flask
7.1.4 Connection of flask to condenser
7.2 Filling of cooling bath
7.3 Adjustment of temperature of sample
8 Procedure [Go to Page]
8.1 Test portion
8.2 Apparatus assembly
8.3 Operating conditions [Go to Page]
8.3.1 General
8.3.2 Materials with boiling point below 150 °C
8.3.3 Materials with boiling point above 150 °C
8.4 Initial boiling point
8.5 Distillation
8.6 Dry point
8.7 End point
8.8 Atmospheric pressure
8.9 Recovery
8.10 Distillation loss
9 Notes on procedure [Go to Page]
9.1 Factors causing superheating
9.2 Flame in contact with the flask
9.3 Application of heat
9.4 Extraneous heat source
9.5 Condition of equipment
9.6 Use of electric heaters
9.7 Safety precautions [Go to Page]
9.7.1 Peroxide formation
9.7.2 Flammability
10 Calculations [Go to Page]
10.1 Thermometer bore correction
10.2 Thermometer bulb shrinkage correction
10.3 Barometer correction
10.4 Combined corrections
10.5 Precision [Go to Page]
10.5.1 General
10.5.2 Repeatability, r
10.5.3 Reproducibility, R
11 Test report
Annex A (normative) Thermometer to be used, normal boiling point and boiling point correction factor
Annex B (informative) Test for peroxides
Bibliography [Go to Page]

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