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eLibrary > BS ISO 334:2013 Solid mineral fuels. Determination of total sulphur. Eschka method >

BS ISO 334:2013 Solid mineral fuels. Determination of total sulphur. Eschka method, 2013

Section sec_1
Section sec_2
Section sec_3
Section sec_4
Section sec_4.1
Section sec_4.2
Section sec_4.3
Section sec_4.4
Section sec_4.5
Section sec_4.6
Section sec_4.7
Section sec_5
Section sec_5.1
Section sec_5.2
Section sec_5.3
Section sec_5.4
Section sec_5.5
Section sec_5.6
Section sec_5.7
Section sec_6
Section sec_7
Section sec_7.1
Section sec_7.1.1
Table tab_1
Section sec_7.1.2
Section sec_7.2
Section sec_7.3
Section sec_7.3.1
Section sec_7.3.2
Section sec_7.4
Section sec_7.5
Section sec_7.6
Section sec_7.7
Section sec_8
Section sec_9
Section sec_9.1
Section sec_9.2
Section sec_10
Annex sec_A
Table tab_A.1
Foreword
Introduction
1 Scope
2 Normative references
3 Principle
4 Reagents
4.1 Eschka mixture
4.2 Hydrochloric acid
4.3 Potassium sulfate solution
4.4 Barium chloride, approximately 85 g/l solution
4.5 Methyl red indicator solution
4.6 Ammonia
4.7 Silver nitrate, 17 g/l solution
5 Apparatus
5.1 Analytical balance
5.2 Graduated glassware
5.3 Electrically heated muffle furnace
5.4 Crucible
5.5 Flat plate
5.6 Gooch crucible
5.7 Air oven
6 Preparation of test sample
7 Procedure
7.1 Test portion
7.2 Charging the crucible
7.3 Ignition
7.4 Recovering the residue
7.5 Extraction
7.6 Precipitation of barium sulfate
7.7 Blank testing
8 Expression of results
9 Precision
9.1 Repeatability limit
9.2 Reproducibility limit
10 Test report
Annex A (informative) Derivation of factors used in the calculation in Clause 8 [Go to Page]

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