1. Scope

1.1 These test methods cover the chemical analysis of tool steels and other similar medium- and high-alloy steels having chemical compositions within the following limits:

1.3 Test methods for the determination of several elements not included in this standard can be found in Test Methods E 30 and Test Methods E 1019.

1.4 Some of the concentration ranges given in are too broad to be covered by a single test method and therefore this standard contains multiple test methods for some elements. The user must select the proper test method by matching the information given in the Scope and Interference sections of each test method with the composition of the alloy to be analyzed.

1.5 The values stated in SI units are to be regarded as standard. In some cases, exceptions allowed in Practice E 380 are also used.

This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section and in special 'Warning' paragraphs throughout these test methods.

1.6 This method covers the determination of manganese in concentrations from 0.10 to 5.00 %.

1.7 This test method covers the determination of phosphorus in concentrations from 0.002 to 0.05 %.

2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

Other Document

ASTM Standards

D1193 Specification for Reagent Water

E29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications

E30 Test Methods for Chemical Analysis of Steel, Cast Iron, Open-Hearth Iron, and Wrought Iron

E50 Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials

E60 Practice for Analysis of Metals, Ores, and Related Materials by Spectrophotometry

E173 Practice for Conducting Interlaboratory Studies of Methods for Chemical Analysis of Metals

E350 Test Methods for Chemical Analysis of Carbon Steel, Low-Alloy Steel, Silicon Electrical Steel, Ingot Iron, and Wrought Iron

E351 Test Methods for Chemical Analysis of Cast Iron--All Types

E353 Test Methods for Chemical Analysis of Stainless, Heat-Resisting, Maraging, and Other Similar Chromium-Nickel-Iron Alloys

E882 Guide for Accountability and Quality Control in the Chemical Analysis Laboratory

E1019 Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel, Iron, Nickel, and Cobalt Alloys by Various Combustion and Fusion Techniques

E1024 Guide for Chemical Analysis of Metals and Metal Bearing Ores by Flame Atomic Absorption Spectrophotometry

E1806 Practice for Sampling Steel and Iron for Determination of Chemical Composition

Keywords

atomic absorption; chromium; cobalt; combustion analysis; copper; gravimetric; high-alloy steel; induction furnace; infrared absorption; ion exchange; lead; nickel; manganese; molybdenum; phosphorus; silicon; spectrophotometric; sulfur; tin; titration; titrimetric; tool steels; total carbon; vanadium;

ICS Code

ICS Number Code 77.040.30 (Chemical analysis of metals)

DOI: 10.1520/E0352-93R06

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