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  • ASTM
    E352-13 Standard Test Methods for Chemical Analysis of Tool Steels and Other Similar Medium- and High-Alloy Steels
    Edition: 2013
    $148.51
    Unlimited Users per year

Description of ASTM-E352 2013

ASTM E352 - 13

Standard Test Methods for Chemical Analysis of Tool Steels and Other Similar Medium- and High-Alloy Steels

Active Standard ASTM E352 | Developed by Subcommittee: E01.01

Book of Standards Volume: 03.05




ASTM E352

Significance and Use

4.1 These test methods for the chemical analysis of metals and alloys are primarily intended as referee methods to test such materials for compliance with compositional specifications particularly those under the jurisdiction of ASTM Committee A1 on Steel, Stainless Steel, and Related Alloys. It is assumed that all who use these test methods will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory under appropriate quality control practices such as those described in Guide E882 .

1. Scope

1.1 These test methods cover the chemical analysis of tool steels and other similar medium- and high-alloy steels having chemical compositions within the following limits:

Element

Composition Range,?%

Aluminum

0.005 to 1.5

Boron

0.001 to 0.10

Carbon

0.03 to 2.50

Chromium

0.10 to 14.0

Cobalt

0.10 to 14.0

Copper

0.01 to 2.0

Lead

0.001 to 0.01

Manganese

0.10 to 15.00

Molybdenum

0.01 to 10.00

Nickel

0.02 to 4.00

Nitrogen

0.001 to 0.20

Phosphorus

0.002 to 0.05

Silicon

0.10 to 2.50

Sulfur

0.002 to 0.40

Tungsten

0.01 to 21.00

Vanadium

0.02 to 5.50


1.2 The test methods in this standard are contained in the sections indicated below:

Sections

Carbon, Total, by the Combustion
Thermal Conductivity Method
Discontinued 1986

Carbon, Total, by the Combustion Gravimetrical
Method Discontinued

Chromium by the Atomic Absorption Method

(0.006 % to 1.00?%)

174

Chromium by the Peroxydisulfate
OxidationTitration Method

(0.10 % to 14.00?%)

184

Chromium by the Peroxydisulfate-Oxidation
Titrimetric Method Discontinued 1980

Cobalt by the Ion-Exchange
Potentiometric Titration Method

(2 % to 14?%)

52

Cobalt by the Nitroso-R-Salt
Spectrophotometric Method

(0.10 % to 5.0?%)

60

Copper by the Neocuproine
Spectrophotometric Method

(0.01 % to 2.00?%)

89

Copper by the Sulfide Precipitation-
Electrodeposition Gravimetric Method

(0.01 % to 2.0?%)

70

Lead by the Ion-ExchangeAtomic
Absorption Method

(0.001 % to 0.01?%)

99

Nickel by the Dimethylglyoxime
Gravimetric Method

(0.1 % to 4.0?%)

144

Manganese by the Periodate
Spectrophotometric Method

(0.10 % to 5.00?%)

8

Molybdenum by the Ion Exchange
8-Hydroxyquinoline Gravimetric Method

203

Molybdenum by the Spectrophotometric Method

(0.01 % to 1.50?%)

162

Phosphorus by the Alkalimetric Method

(0.01 % to 0.05?%)

136

Phosphorus by the Molybdenum Blue
Spectrophotometric Method

(0.002 % to 0.05?%)

18

Silicon by the Gravimetric Method

(0.10 % to 2.50?%)

45

Sulfur by the Gravimetric
Method Discontinued 1988

Sulfur by the Combustion-Iodate
Titration Method Discontinued

Sulfur by the Chromatographic
Gravimetric Method Discontinued 1980

Tin by the Solvent Extraction
Atomic Absorption Method

(0.002 % to 0.10?%)

152

Vanadium by the Atomic
Absorption Method

(0.006 % to 0.15?%)

193


1.3 Test methods for the determination of carbon and sulfur not included in this standard can be found in Test Methods E1019 .

1.4 Some of the composition ranges given in 1.1 are too broad to be covered by a single test method and therefore this standard contains multiple test methods for some elements. The user must select the proper test method by matching the information given in the Scope and Interference sections of each test method with the composition of the alloy to be analyzed.

1.5 The values stated in SI units are to be regarded as standard.

1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 6 and in special Warning paragraphs throughout these test methods.


2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

Other Document

ISO?5725 Precision of Test Methods--Determination of Repeatability and Reproducibility for Inter-Laboratory Tests

ASTM Standards

D1193 Specification for Reagent Water

E29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications

E30 Test Methods for Chemical Analysis of Steel, Cast Iron, Open-Hearth Iron, and Wrought Iron

E50 Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials

E60 Practice for Analysis of Metals, Ores, and Related Materials by Spectrophotometry

E173 Practice for Conducting Interlaboratory Studies of Methods for Chemical Analysis of Metals

E350 Test Methods for Chemical Analysis of Carbon Steel, Low-Alloy Steel, Silicon Electrical Steel, Ingot Iron, and Wrought Iron

E351 Test Methods for Chemical Analysis of Cast Iron--All Types

E353 Test Methods for Chemical Analysis of Stainless, Heat-Resisting, Maraging, and Other Similar Chromium-Nickel-Iron Alloys

E882 Guide for Accountability and Quality Control in the Chemical Analysis Laboratory

E1019 Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel, Iron, Nickel, and Cobalt Alloys by Various Combustion and Fusion Techniques

E1024 Guide for Chemical Analysis of Metals and Metal Bearing Ores by Flame Atomic Absorption Spectrophotometry

E1806 Practice for Sampling Steel and Iron for Determination of Chemical Composition


Keywords

atomic absorption; chromium; cobalt; combustion analysis; copper; gravimetric; high-alloy steel; induction furnace; infrared absorption; ion exchange; lead; nickel; manganese; molybdenum; phosphorus; silicon; spectrophotometric; sulfur; tin; titration; titrimetric; tool steels; total carbon; vanadium;


ICS Code

ICS Number Code 77.040.30 (Chemical analysis of metals)


DOI: 10.1520/E0352-13

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ASTM E352

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