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  • ASTM
    E350-12 Standard Test Methods for Chemical Analysis of Carbon Steel, Low-Alloy Steel, Silicon Electrical Steel, Ingot Iron, and Wrought Iron
    Edition: 2012
    $172.22
    Unlimited Users per year

Description of ASTM-E350 2012

ASTM E350 - 12

Standard Test Methods for Chemical Analysis of Carbon Steel, Low-Alloy Steel, Silicon Electrical Steel, Ingot Iron, and Wrought Iron

Active Standard ASTM E350 | Developed by Subcommittee: E01.01

Book of Standards Volume: 03.05



Translated Standard: Russian
more info


ASTM E350

Significance and Use

These test methods for the chemical analysis of metals and alloys are primarily intended as referee methods to test such materials for compliance with compositional specifications, particularly those under the jurisdiction of ASTM Committees A01 on Steel, Stainless Steel, and Related Alloys and A04 on Iron Castings. It is assumed that all who use these test methods will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory under appropriate quality control practices such as those described in Guide E882 .

1. Scope

1.1 These test methods cover the chemical analysis of carbon steels, low-alloy steels, silicon electrical steels, ingot iron, and wrought iron having chemical compositions within the following limits:

Element Composition Range, %
Aluminum 0.001 to 1.50
Antimony 0.002 to 0.03
Arsenic 0.0005 to 0.10
Bismuth 0.005 to 0.50
Boron 0.0005 to 0.02
Calcium 0.0005 to 0.01
Cerium 0.005 to 0.50
Chromium 0.005 to 3.99
Cobalt 0.01 to 0.30
Columbium (Niobium) 0.002 to 0.20
Copper 0.005 to 1.50
Lanthanum 0.001 to 0.30
Lead 0.001 to 0.50
Manganese 0.01 to 2.50
Molybdenum 0.002 to 1.50
Nickel 0.005 to 5.00
Nitrogen 0.0005 to 0.04
Oxygen 0.0001 to 0.03
Phosphorus 0.001 to 0.25
Selenium 0.001 to 0.50
Silicon 0.001 to 5.00
Sulfur 0.001 to 0.60
Tin 0.002 to 0.10
Titanium 0.002 to 0.60
Tungsten 0.005 to 0.10
Vanadium 0.005 to 0.50
Zirconium 0.005 to 0.15

1.2 The test methods in this standard are contained in the sections indicated as follows:

Sections
Aluminum, Total, by the 8-Quinolinol Gravimetric Method
(0.20 % to 1.5 %) 		124 131
Aluminum, Total, by the 8-Quinolinol Spectrophotometric
Method (0.003 % to 0.20 %) 		76 86
Aluminum, Total or Acid-Soluble, by the Atomic Absorption
Spectrometry Method (0.005 % to 0.20 %) 		308 317
Antimony by the Brilliant Green Spectrophotometric
Method (0.0002 % to 0.030 %) 		142 151
Bismuth by the Atomic Absorption Spectrometry
Method (0.02 % to 0.25 %) 		298 307
Boron by the Distillation-Curcumin Spectrophotometric
Method (0.0003 % to 0.006 %) 		208 219
Calcium by the Direct-Current Argon Plasma Atomic
Emission Spectroscopy Method (0.0005 % to 0.010 %) 		289 297
Carbon, Total, by the Combustion Gravimetric Method
(0.05 % to1.80 %) Discontinued 1995
Cerium and Lanthanum by the Direct Current Plasma
Atomic Emission Spectrometry Method
(0.003 % to 0.50 % Cerium, 0.001 % to 0.30 % Lanthanum) 		249 257
Chromium by the Atomic Absorption Spectrometry
Method (0.006 % to 1.00 %) 		220 229
Chromium by the Peroxydisulfate Oxidation-Titration
Method (0.05 % to 3.99 %) 		230 238
Cobalt by the Nitroso-R Salt Spectrophotometric
Method (0.01 % to 0.30 %) 		53 62
Copper by the Atomic Absorption Spectrometry
Method (0.004 % to 0.5 %) 		279 288
Copper by the Neocuproine Spectrophotometric
Method (0.005 % to 1.50 %) 		114 123
Lead by the Ion-Exchange Atomic Absorption Spectrometry
Method (0.001 % to 0.50 %) 		132 141
Manganese by the Atomic Absorption Spectrometry
Method (0.005 % to 2.0 %) 		269 278
Manganese by the Metaperiodate Spectrophotometric
Method (0.01 % to 2.5 %) 		9-18
Manganese by the Peroxydisulfate-Arsenite Titrimetric
Method(0.10 % to 2.50 %) 		164 171
Molybdenum by the Thiocyanate Spectrophotometric
Method (0.01 % to 1.50 %) 		152 163
Nickel by the Atomic Absorption Spectrometry
Method (0.003 % to 0.5 %) 		318 327
Nickel by the Dimethylglyoxime Gravimetric
Method (0.1 % to 5.00 %) 		180 187
Nickel by the Ion-Exchange-Atomic-Absorption Spectrometry
Method (0.005 % to 1.00 %) 		188 197
Phosphorus by the Alkalimetric Method
(0.02 % to 0.25 %) 		172 179
Phosphorus by the Molybdenum Blue Spectrophotometric
Method (0.003 % to 0.09 %) 		19-30
Silicon by the Molybdenum Blue Spectrophotometric
Method (0.01 % to 0.06 %) 		103 113
Silicon by the Gravimetric Titration
Method (0.05 % to 3.5 %) 		46 52
Sulfur by the Combustion-Iodate Titration Method
(0.005 % to 0.3 %) 		37 45
Tin by the Sulfide-Iodometric Titration
Method (0.01 % to 0.1 %) 		95 102
Tin by the Solvent Extraction-Atomic Absorption Spectrometry Method
(0.002 % to 0.10 %) 		198 207
Titanium, Total, by the Diantipyrylmethane Spectrophotometric
Method (0.025 % to 0.30 %) 		258 268
Vanadium by the Atomic Absorption Spectrometry
Method (0.006 % to 0.15 %) 		239 248

1.3 Test methods for the determination of several elements not included in this standard can be found in Test Methods E1019 .

1.4 Some of the composition ranges given in 1.1 are too broad to be covered by a single test method and therefore this standard contains multiple test methods for some elements. The user must select the proper test method by matching the information given in the Scope and Interference sections of each test method with the composition of the alloy to be analyzed.

1.5 The values stated in SI units are to be regarded as standard. In some cases, exceptions allowed in are also used.

1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 6 and in special Warning paragraphs throughout these test methods.


2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

ASTM Standards

D1193 Specification for Reagent Water

E29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications

E30 Test Methods for Chemical Analysis of Steel, Cast Iron, Open-Hearth Iron, and Wrought Iron

E50 Practices for Apparatus, Reagents, and Safety Considerations for Chemical Analysis of Metals, Ores, and Related Materials

E60 Practice for Analysis of Metals, Ores, and Related Materials by Spectrophotometry

E173 Practice for Conducting Interlaboratory Studies of Methods for Chemical Analysis of Metals

E319 Practice for the Evaluation of Single-Pan Mechanical Balances

E351 Test Methods for Chemical Analysis of Cast Iron--All Types

E352 Test Methods for Chemical Analysis of Tool Steels and Other Similar Medium- and High-Alloy Steels

E353 Test Methods for Chemical Analysis of Stainless, Heat-Resisting, Maraging, and Other Similar Chromium-Nickel-Iron Alloys

E354 Test Methods for Chemical Analysis of High-Temperature, Electrical, Magnetic, and Other Similar Iron, Nickel, and Cobalt Alloys

E882 Guide for Accountability and Quality Control in the Chemical Analysis Laboratory

E1019 Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel, Iron, Nickel, and Cobalt Alloys by Various Combustion and Fusion Techniques

E1024 Guide for Chemical Analysis of Metals and Metal Bearing Ores by Flame Atomic Absorption Spectrophotometry

E1097 Guide for Determination of Various Elements by Direct Current Plasma Atomic Emission Spectrometry

E1806 Practice for Sampling Steel and Iron for Determination of Chemical Composition

ISO Standard

ISO5725 Precision of Test Methods--Determination of Repeatability and Reproducibility for Inter-Laboratory Tests

Keywords


ICS Code

ICS Number Code 77.040.30 (Chemical analysis of metals)


DOI: 10.1520/E0350-12

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ASTM E350

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