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  • ASTM
    D5368-13 Standard Test Methods for Gravimetric Determination of Total Solvent Extractable Content (TSEC) of Solid Waste Samples (Redline)
    Edition: 2013
    $62.90
    Unlimited Users per year

Description of ASTM-D5368 2013

ASTM D5368 - 13

Standard Test Methods for Gravimetric Determination of Total Solvent Extractable Content (TSEC) of Solid Waste Samples

Active Standard ASTM D5368 | Developed by Subcommittee: D34.01.06

Book of Standards Volume: 11.04




ASTM D5368

Significance and Use

5.1 The TSEC provides a quantitative measure of the total solvent extractable organic content of the solid waste in question. Based upon the TSEC, the extract may be analyzed or further processed (that is, further cleanup or solvent concentration) in preparation for analysis. Thus, the TSEC provides a quantitative measure for optimizing the extractable organic concentration prior to chemical analysis.

5.2 The TSEC of soil or waste material may be used as a quantitative measure for the screening and selection of samples for chemical analysis.

5.3 The TSEC may be useful as a simple and relatively inexpensive quantitative indicator of changes occurring in the total extractable organic content of soil or waste materials.

5.4 The detection limit of the TSEC depends upon the specific procedures employed. Typical detection limits in solvent extracts (that is, without solvent pre-concentration) for Method A are more than 1000 ?g/g. For Method B typical detection limits are 20 to 100 ?g/g in the solvent extract. For Method C the typical detection limits are 3 to 20 ?g/g for solutes in the solvent extract.

5.5 The sensitivity of the methods can be adjusted by varying the volume of solvent extract prior to gravimetric residue determination.

1. Scope

1.1 These test methods describe standard procedures for gravimetrically determining the total nonvolatile and semi-volatile organic content of solvent extracts from soils or solid wastes. The following methods are included:

Section

Method AMicro-Determination of TSEC

11- 13

Method BEvaporating Dish Procedure

14- 16

Method CBoiling Flask Procedure

17- 19


1.2 These methods are used after a solvent extract is obtained from a soil or solid waste. For these methods to be applicable, the extraction solvent must have a boiling point less than that of water at ambient pressure.

1.3 The total solvent extractable content (TSEC) of a soil, sediment, sludge, or solid waste depends upon the solvent and method used for the extraction procedure.


2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

ASTM Standards

D2109 Test Methods for Nonvolatile Matter in Halogenated Organic Solvents and Their Admixtures

D2910 Method for Removal of Organic Matter from Water by Activated Carbon Absorption

D3086 Test Method for Organochlorine Pesticides in Water

D3445 Method of Test for Nonvolatile Matter in Trichlorotrifluoroethane

D3694 Practices for Preparation of Sample Containers and for Preservation of Organic Constituents

D4281 Test Method for Oil and Grease (Fluorocarbon Extractable Substances) by Gravimetric Determination

D5369 Practice for Extraction of Solid Waste Samples for Chemical Analysis Using Soxhlet Extraction


Keywords


ICS Code

ICS Number Code 13.030.10 (Solid wastes)


DOI: 10.1520/D5368-13

ASTM International is a member of CrossRef.

ASTM D5368

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ASTM International, formerly known as the American Society for Testing and Materials (ASTM), is a globally recognized leader in the development and delivery of international voluntary consensus standards. Today, some 12,000 ASTM standards are used around the world to improve product quality, enhance safety, facilitate market access and trade, and build consumer confidence. ASTM’s leadership in international standards development is driven by the contributions of its members: more than 30,000 of the world’s top technical experts and business professionals representing 150 countries. Working in an open and transparent process and using ASTM’s advanced electronic infrastructure, ASTM members deliver the test methods, specifications, guides, and practices that support industries and governments worldwide.
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